Crystallography Open Database

Information card for entry 7022038

7022037 << 7022038 >> 7022039

Preview

Coordinates	7022038.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H60 Li4 N4 Si4
Calculated formula	C52 H60 Li4 N4 Si4
Title of publication	LiCl-effect on asymmetric intramolecular hydroamination catalyzed by binaphthylamido yttrium complexes.
Authors of publication	Chapurina, Yulia; Guillot, Régis; Lyubov, Dmitrii; Trifonov, Alexander; Hannedouche, Jérôme; Schulz, Emmanuelle
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	2
Pages of publication	507 - 520
a	23.2936 ± 0.0007 Å
b	10.2146 ± 0.0003 Å
c	22.5327 ± 0.0007 Å
α	90°
β	111.314 ± 0.001°
γ	90°
Cell volume	4994.6 ± 0.3 Å³
Cell temperature	100 ± 1 K
Ambient diffraction temperature	100 ± 1 K
Number of distinct elements	5
Space group number	5
Hermann-Mauguin space group symbol	C 1 2 1
Hall space group symbol	C 2y
Residual factor for all reflections	0.0475
Residual factor for significantly intense reflections	0.0441
Weighted residual factors for significantly intense reflections	0.1123
Weighted residual factors for all reflections included in the refinement	0.1149
Goodness-of-fit parameter for all reflections included in the refinement	1.062
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7022038.cif
89950	2013-11-17	cif/ Adding structures of 7022036, 7022037, 7022038, 7022039, 7022040 via cif-deposit CGI script.	7022038.cif