Crystallography Open Database

Information card for entry 7023243

Preview

Coordinates	7023243.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H37 N2 O8 P3 S10 W3
Calculated formula	C18 H37 N2 O7.99 P3 S10 W3
Title of publication	Tungsten and molybdenum incomplete cuboidal clusters; kinetico-mechanistic studies and association in dimers.
Authors of publication	Hernandez-Molina, Rita; Gushchin, Artem; González-Platas, Javier; Martínez, Manuel; Rodríguez, Carlos; Vicent, Cristian
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	42
Pages of publication	15016 - 15027
a	10.71 ± 0.001 Å
b	13.889 ± 0.001 Å
c	15.587 ± 0.001 Å
α	67.158 ± 0.001°
β	82.468 ± 0.001°
γ	81.623 ± 0.001°
Cell volume	2106.9 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0575
Residual factor for significantly intense reflections	0.047
Weighted residual factors for significantly intense reflections	0.1296
Weighted residual factors for all reflections included in the refinement	0.1369
Goodness-of-fit parameter for all reflections included in the refinement	1.221
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179937 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/32.	7023243.cif
90478	2013-11-17	cif/ Adding structures of 7023242, 7023243, 7023244, 7023245 via cif-deposit CGI script.	7023243.cif