Crystallography Open Database

Information card for entry 7023446

Preview

Coordinates	7023446.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H24 Cu11 N54 O12
Calculated formula	C36 H24 Cu11 N54 O12
Title of publication	Rung-defected ladder of azido-bridged Cu(II) chains linked by [Cu(picolinate)2] units.
Authors of publication	Liu, Jiang; Qin, Ying-Lian; Qu, Mei; Clérac, Rodolphe; Zhang, Xian-Ming
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	32
Pages of publication	11571 - 11575
a	11.05 ± 0.003 Å
b	12.255 ± 0.004 Å
c	13.652 ± 0.004 Å
α	94.145 ± 0.007°
β	106.864 ± 0.006°
γ	107.51 ± 0.005°
Cell volume	1661.3 ± 0.9 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1534
Residual factor for significantly intense reflections	0.0793
Weighted residual factors for significantly intense reflections	0.1708
Weighted residual factors for all reflections included in the refinement	0.228
Goodness-of-fit parameter for all reflections included in the refinement	0.98
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179939 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/34.	7023446.cif
90538	2013-11-18	cif/ Adding structures of 7023446 via cif-deposit CGI script.	7023446.cif