Crystallography Open Database

Information card for entry 7023808

Preview

Coordinates	7023808.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C186 H126 F30 N31 O3 P5 Ru3
Calculated formula	C186 H126 F3 N31 O3 P5.3 Ru3
Title of publication	Multi-pyridine decorated Fe(ii) and Ru(ii) complexes by Pd(0)-catalysed cross couplings: new building blocks for metallosupramolecular assemblies.
Authors of publication	Yang, Jiajia; Clegg, Jack K.; Jiang, Qibai; Lui, Xiaoming; Yan, Hong; Zhong, Wei; Beves, Jonathon E.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	44
Pages of publication	15625 - 15636
a	19.323 ± 0.005 Å
b	20.548 ± 0.006 Å
c	26.542 ± 0.007 Å
α	81.138 ± 0.005°
β	81.923 ± 0.005°
γ	84.253 ± 0.005°
Cell volume	10276 ± 5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1947
Residual factor for significantly intense reflections	0.1204
Weighted residual factors for significantly intense reflections	0.3256
Weighted residual factors for all reflections included in the refinement	0.3787
Goodness-of-fit parameter for all reflections included in the refinement	1.289
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179943 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/38.	7023808.cif
90643	2013-11-18	cif/ Adding structures of 7023805, 7023806, 7023807, 7023808 via cif-deposit CGI script.	7023808.cif