Crystallography Open Database

Information card for entry 7024025

Preview

Coordinates	7024025.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H81 Fe9 N16 Na9 O123 Si3 W28
Calculated formula	C30 H58 Fe9 N10 Na5 O123 Si3 W28
Title of publication	Preparation of polyoxometalates in ionic liquids by ionothermal synthesis.
Authors of publication	Lin, Shiwei; Liu, Wenli; Li, Yangguang; Wu, Qiong; Wang, Enbo; Zhang, Zhiming
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	7
Pages of publication	1740 - 1744
a	15.302 ± 0.003 Å
b	23.309 ± 0.005 Å
c	27.828 ± 0.006 Å
α	86.25 ± 0.03°
β	89.04 ± 0.03°
γ	89.28 ± 0.03°
Cell volume	9902 ± 4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1575
Residual factor for significantly intense reflections	0.0857
Weighted residual factors for significantly intense reflections	0.1799
Weighted residual factors for all reflections included in the refinement	0.2132
Goodness-of-fit parameter for all reflections included in the refinement	0.937
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179945 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/40.	7024025.cif
92031	2014-01-12	cif/ Adding structures of 7024025, 7024026 via cif-deposit CGI script.	7024025.cif