Crystallography Open Database

Information card for entry 7024400

Preview

Coordinates	7024400.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H46 Cl12 N12 Pd
Calculated formula	C27 H46 Cl12 N12 Pd
Title of publication	Coordination of neutral, methylene bridged bis-guanidyls at palladium.
Authors of publication	Khalaf, Majid S.; Oakley, Sarah H.; Coles, Martyn P.; Hitchcock, Peter B.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	6
Pages of publication	1635 - 1642
a	11.2121 ± 0.0003 Å
b	17.9696 ± 0.0007 Å
c	22.7166 ± 0.0008 Å
α	90°
β	96.199 ± 0.002°
γ	90°
Cell volume	4550.1 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0791
Residual factor for significantly intense reflections	0.0496
Weighted residual factors for significantly intense reflections	0.1223
Weighted residual factors for all reflections included in the refinement	0.1452
Goodness-of-fit parameter for all reflections included in the refinement	1.088
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179949 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/44.	7024400.cif
92471	2014-01-12	cif/ Adding structures of 7024396, 7024397, 7024398, 7024399, 7024400 via cif-deposit CGI script.	7024400.cif