Crystallography Open Database

Information card for entry 7024669

Preview

Coordinates	7024669.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47.75 H55.75 Al2 Cl8.25 N3
Calculated formula	C47 H55 Al2 Cl6 N3
Title of publication	Disproportionation and radical formation in the coordination of "GaI" with bis(imino)pyridines.
Authors of publication	Jurca, Titel; Dawson, Karl; Mallov, Ian; Burchell, Tara; Yap, Glenn P. A.; Richeson, Darrin S.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	5
Pages of publication	1266 - 1272
a	15.124 ± 0.004 Å
b	18.054 ± 0.005 Å
c	22.939 ± 0.006 Å
α	90°
β	90°
γ	90°
Cell volume	6263 ± 3 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	5
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0923
Residual factor for significantly intense reflections	0.0657
Weighted residual factors for significantly intense reflections	0.1869
Weighted residual factors for all reflections included in the refinement	0.2066
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179951 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/46.	7024669.cif
92630	2014-01-12	cif/ Adding structures of 7024666, 7024667, 7024668, 7024669 via cif-deposit CGI script.	7024669.cif