Crystallography Open Database

Information card for entry 7024707

Preview

Coordinates	7024707.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H28 N P2 Te2 Tl
Calculated formula	C12 H28 N P2 Te2 Tl
Title of publication	Thallium(I) complexes of dichalcogenido imidodiphosphinates {Tl[(EP(i)Pr(2))(2)N]}(n) (E = Te, Se, S): Synthesis, NMR spectra and a structural comparison.
Authors of publication	Ritch, Jamie S.; Chivers, Tristram
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	7
Pages of publication	1745 - 1750
a	9.301 ± 0.0019 Å
b	15.571 ± 0.003 Å
c	16.289 ± 0.003 Å
α	116.29 ± 0.03°
β	98.64 ± 0.03°
γ	100.7 ± 0.03°
Cell volume	2004.6 ± 1 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0518
Residual factor for significantly intense reflections	0.0381
Weighted residual factors for significantly intense reflections	0.0864
Weighted residual factors for all reflections included in the refinement	0.0929
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179952 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/47.	7024707.cif
92645	2014-01-12	cif/ Adding structures of 7024707, 7024708, 7024709 via cif-deposit CGI script.	7024707.cif