Crystallography Open Database

Information card for entry 7024709

Preview

Coordinates	7024709.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H28 N P2 S2 Tl
Calculated formula	C12 H28 N P2 S2 Tl
Title of publication	Thallium(I) complexes of dichalcogenido imidodiphosphinates {Tl[(EP(i)Pr(2))(2)N]}(n) (E = Te, Se, S): Synthesis, NMR spectra and a structural comparison.
Authors of publication	Ritch, Jamie S.; Chivers, Tristram
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	7
Pages of publication	1745 - 1750
a	8.3507 ± 0.0017 Å
b	9.2269 ± 0.0018 Å
c	13.319 ± 0.003 Å
α	108.92 ± 0.03°
β	98.79 ± 0.03°
γ	104.88 ± 0.03°
Cell volume	906.4 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0314
Residual factor for significantly intense reflections	0.0299
Weighted residual factors for significantly intense reflections	0.0788
Weighted residual factors for all reflections included in the refinement	0.0804
Goodness-of-fit parameter for all reflections included in the refinement	1.056
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179952 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/47.	7024709.cif
92645	2014-01-12	cif/ Adding structures of 7024707, 7024708, 7024709 via cif-deposit CGI script.	7024709.cif