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Information card for entry 7024867
Preview
| Coordinates | 7024867.cif |
|---|---|
| Original paper (by DOI) | HTML |
| External links | PubChem |
| Formula | C18 H26 N O5 P S Si2 W |
|---|---|
| Calculated formula | C18 H26 N O5 P S Si2 W |
| Title of publication | Novel access to azaphosphiridine complexes and first applications using Brønsted acid-induced ring expansion reactions. |
| Authors of publication | Fankel, Stefan; Helten, Holger; von Frantzius, Gerd; Schnakenburg, Gregor; Daniels, Jörg; Chu, Victoria; Müller, Christina; Streubel, Rainer |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2010 |
| Journal volume | 39 |
| Journal issue | 14 |
| Pages of publication | 3472 - 3481 |
| a | 9.3006 ± 0.0004 Å |
| b | 9.8061 ± 0.0004 Å |
| c | 15.3241 ± 0.0006 Å |
| α | 72.925 ± 0.003° |
| β | 75.155 ± 0.003° |
| γ | 77.227 ± 0.003° |
| Cell volume | 1275.21 ± 0.09 Å3 |
| Cell temperature | 123 ± 2 K |
| Ambient diffraction temperature | 123 ± 2 K |
| Number of distinct elements | 8 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0358 |
| Residual factor for significantly intense reflections | 0.0323 |
| Weighted residual factors for significantly intense reflections | 0.0842 |
| Weighted residual factors for all reflections included in the refinement | 0.0851 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.043 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301848 (current) | 2025-08-21 | Add cross-references to PubChem compounds in COD range 7/02/ Each referenced PubChem compound corresponds to the full crystal structure. |
7024867.cif |
| 179953 | 2016-03-25 | cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/48. |
7024867.cif |
| 92720 | 2014-01-12 | cif/ Adding structures of 7024864, 7024865, 7024866, 7024867, 7024868 via cif-deposit CGI script. |
7024867.cif |
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Users of the data should acknowledge the original authors of the
structural data.