Crystallography Open Database

Information card for entry 7024898

Preview

Coordinates	7024898.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H45 B2 Br P2 Si2 Sn
Calculated formula	C19 H45 B2 Br P2 Si2 Sn
SMILES	[Sn](Br)([C@H]([P]([BH3])(C)C)[Si](C)(C)C)([C@H]([P]([BH3])(C)C)[Si](C)(C)C)Cc1ccccc1
Title of publication	Oxidation reactions of a phosphine-borane-stabilised dialkylstannylene.
Authors of publication	Wills, Corinne; Izod, Keith; Clegg, William; Harrington, Ross W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	9
Pages of publication	2379 - 2384
a	9.211 ± 0.003 Å
b	9.917 ± 0.004 Å
c	32.443 ± 0.009 Å
α	90°
β	90°
γ	90°
Cell volume	2963.5 ± 1.7 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0472
Residual factor for significantly intense reflections	0.0327
Weighted residual factors for significantly intense reflections	0.0521
Weighted residual factors for all reflections included in the refinement	0.0552
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179953 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/48.	7024898.cif
92729	2014-01-12	cif/ Adding structures of 7024896, 7024897, 7024898 via cif-deposit CGI script.	7024898.cif