Crystallography Open Database

Information card for entry 7025183

Preview

Coordinates	7025183.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H44 Cl4 N2 P2 Si2 Zn2
Calculated formula	C32 H44 Cl4 N2 P2 Si2 Zn2
SMILES	c1(ccccc1)P(c1ccccc1)(=[N]([Si](C)(C)C)[Zn]1([Cl][Zn]([N](=P(c2ccccc2)(c2ccccc2)C)[Si](C)(C)C)([Cl]1)Cl)Cl)C
Title of publication	Reactivity of Zn(II), Mg(II) and Al(III) chlorides with a phosphinimine ligand: new tetrameric inverse crown ether structures.
Authors of publication	Valerio Cárdenas, Cintya; Muñoz Hernández, Miguel Angel; Grévy, Jean-Michel
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	28
Pages of publication	6441 - 6448
a	8.6601 ± 0.0011 Å
b	11.2147 ± 0.0013 Å
c	11.4194 ± 0.0014 Å
α	74.417 ± 0.003°
β	74.331 ± 0.002°
γ	69.169 ± 0.002°
Cell volume	979.5 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0533
Residual factor for significantly intense reflections	0.0459
Weighted residual factors for significantly intense reflections	0.1037
Weighted residual factors for all reflections included in the refinement	0.1076
Goodness-of-fit parameter for all reflections included in the refinement	1.073
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179956 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/51.	7025183.cif
92873	2014-01-12	cif/ Adding structures of 7025183, 7025184, 7025185, 7025186, 7025187, 7025188 via cif-deposit CGI script.	7025183.cif