#------------------------------------------------------------------------------
#$Date: 2016-03-25 16:15:23 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179960 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/54/7025414.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7025414
loop_
_publ_author_name
'Arii, Hidekazu'
'Takahashi, Makiko'
'Nanjo, Masato'
'Mochida, Kunio'
_publ_section_title
;
 Syntheses of mono- and dinuclear silylplatinum complexes bearing a
 diphosphino ligand via stepwise bond activation of unsymmetric disilanes.
;
_journal_issue                   28
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              6434
_journal_page_last               6440
_journal_paper_doi               10.1039/c000545b
_journal_volume                  39
_journal_year                    2010
_chemical_formula_sum            'C48 H52 P2 Pt Si2'
_chemical_formula_weight         942.11
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 101.692(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   9.2600(4)
_cell_length_b                   41.553(2)
_cell_length_c                   11.4170(6)
_cell_measurement_reflns_used    34573
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      27.97
_cell_measurement_theta_min      2.07
_cell_volume                     4301.9(4)
_computing_cell_refinement       'HKL Scalepack'
_computing_data_collection       'DIP Image plate'
_computing_data_reduction        'maXus (Mackay et al., 1999)'
_computing_molecular_graphics    'Ortep (Johnson, 1976)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 0.887
_diffrn_measured_fraction_theta_max 0.887
_diffrn_measurement_device_type  KappaCCD
_diffrn_measurement_method       IP
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.090
_diffrn_reflns_av_sigmaI/netI    0.0590
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       54
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            34573
_diffrn_reflns_theta_full        27.97
_diffrn_reflns_theta_max         27.97
_diffrn_reflns_theta_min         2.07
_exptl_absorpt_coefficient_mu    3.424
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.455
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             1904
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.903
_refine_diff_density_min         -3.023
_refine_diff_density_rms         0.196
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.075
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     481
_refine_ls_number_reflns         9176
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.075
_refine_ls_R_factor_all          0.0780
_refine_ls_R_factor_gt           0.0568
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0838P)²+8.1255P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1354
_refine_ls_wR_factor_ref         0.1496
_reflns_number_gt                7216
_reflns_number_total             9176
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c000545b.txt
_cod_data_source_block           complex2b
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      'P 21/n '
_cod_database_code               7025414
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pt1 Pt 0.10452(3) 0.162468(5) 0.91001(2) 0.02493(9) Uani 1 1 d .
H1 H 0.172(9) 0.1740(18) 1.032(9) 0.030 Uiso 1 1 d .
P1 P 0.19453(18) 0.20633(4) 0.82484(17) 0.0263(3) Uani 1 1 d .
P2 P 0.00185(17) 0.14740(4) 0.71851(15) 0.0242(3) Uani 1 1 d .
Si1 Si 0.02952(19) 0.11957(4) 1.02075(17) 0.0246(3) Uani 1 1 d .
Si2 Si 0.2433(2) 0.09375(4) 1.12759(18) 0.0286(4) Uani 1 1 d .
C1 C 0.1594(7) 0.20014(15) 0.6621(7) 0.0307(14) Uani 1 1 d .
H1A H 0.1568 0.2206 0.6224 0.037 Uiso 1 1 d R
H1B H 0.2367 0.1872 0.6421 0.037 Uiso 1 1 d R
C2 C 0.0110(8) 0.18273(15) 0.6209(7) 0.0309(14) Uani 1 1 d .
H2A H 0.0029 0.1755 0.5399 0.037 Uiso 1 1 d R
H2B H -0.0688 0.1971 0.6253 0.037 Uiso 1 1 d R
C3 C 0.3893(7) 0.21662(16) 0.8654(7) 0.0312(14) Uani 1 1 d .
C4 C 0.4490(8) 0.24071(18) 0.8009(9) 0.0395(17) Uani 1 1 d .
H4 H 0.3861 0.2521 0.7371 0.047 Uiso 1 1 d R
C5 C 0.5986(9) 0.2480(2) 0.8300(11) 0.051(2) Uani 1 1 d .
H5 H 0.6373 0.2649 0.7877 0.062 Uiso 1 1 d R
C6 C 0.6897(9) 0.2309(2) 0.9207(11) 0.057(3) Uani 1 1 d .
H6 H 0.7931 0.2358 0.9410 0.068 Uiso 1 1 d R
C7 C 0.6349(10) 0.2074(2) 0.9806(10) 0.054(2) Uani 1 1 d .
H7 H 0.6992 0.1953 1.0416 0.065 Uiso 1 1 d R
C8 C 0.4820(9) 0.1996(2) 0.9554(8) 0.0422(18) Uani 1 1 d .
H8 H 0.4419 0.1830 0.9980 0.051 Uiso 1 1 d R
C9 C 0.1023(7) 0.24390(15) 0.8482(7) 0.0288(13) Uani 1 1 d .
C10 C 0.0133(8) 0.26165(16) 0.7562(7) 0.0341(15) Uani 1 1 d .
H10 H 0.0013 0.2544 0.6749 0.041 Uiso 1 1 d R
C11 C -0.0573(9) 0.28937(18) 0.7825(9) 0.0412(18) Uani 1 1 d .
H11 H -0.1202 0.3012 0.7199 0.049 Uiso 1 1 d R
C12 C -0.0379(8) 0.30031(16) 0.8992(8) 0.0371(16) Uani 1 1 d .
H12 H -0.0852 0.3198 0.9167 0.045 Uiso 1 1 d R
C13 C 0.0508(10) 0.28290(18) 0.9929(9) 0.0434(19) Uani 1 1 d .
H13 H 0.0641 0.2907 1.0736 0.052 Uiso 1 1 d R
C14 C 0.1185(9) 0.25498(18) 0.9658(8) 0.0377(16) Uani 1 1 d .
H14 H 0.1771 0.2430 1.0302 0.045 Uiso 1 1 d R
C15 C 0.0956(7) 0.11532(14) 0.6534(6) 0.0262(12) Uani 1 1 d .
C16 C 0.1836(7) 0.09383(15) 0.7336(7) 0.0310(14) Uani 1 1 d .
H16 H 0.2000 0.0977 0.8182 0.037 Uiso 1 1 d R
C17 C 0.2461(8) 0.06743(16) 0.6891(8) 0.0355(16) Uani 1 1 d .
H17 H 0.3022 0.0521 0.7429 0.043 Uiso 1 1 d R
C18 C 0.2284(8) 0.06248(17) 0.5653(8) 0.0388(17) Uani 1 1 d .
H18 H 0.2713 0.0439 0.5360 0.047 Uiso 1 1 d R
C19 C 0.1480(8) 0.08483(18) 0.4872(8) 0.0379(16) Uani 1 1 d .
H19 H 0.1390 0.0822 0.4025 0.046 Uiso 1 1 d R
C20 C 0.0801(8) 0.11094(17) 0.5315(7) 0.0327(15) Uani 1 1 d .
H20 H 0.0230 0.1260 0.4773 0.039 Uiso 1 1 d R
C21 C -0.1933(7) 0.13766(14) 0.6793(6) 0.0266(12) Uani 1 1 d .
C22 C -0.2534(7) 0.11369(16) 0.5997(7) 0.0293(13) Uani 1 1 d .
H22 H -0.1897 0.1002 0.5642 0.035 Uiso 1 1 d R
C23 C -0.4066(7) 0.10934(15) 0.5725(7) 0.0288(13) Uani 1 1 d .
H23 H -0.4489 0.0926 0.5183 0.035 Uiso 1 1 d R
C24 C -0.4975(7) 0.12842(15) 0.6231(7) 0.0300(14) Uani 1 1 d .
H24 H -0.6024 0.1256 0.6019 0.036 Uiso 1 1 d R
C25 C -0.4383(8) 0.15186(17) 0.7048(8) 0.0355(15) Uani 1 1 d .
H25 H -0.5020 0.1651 0.7411 0.043 Uiso 1 1 d R
C26 C -0.2859(8) 0.15666(16) 0.7339(7) 0.0324(14) Uani 1 1 d .
H26 H -0.2440 0.1727 0.7913 0.039 Uiso 1 1 d R
C27 C -0.0970(7) 0.08759(15) 0.9353(7) 0.0284(13) Uani 1 1 d .
C28 C -0.0414(8) 0.05948(16) 0.8906(7) 0.0345(15) Uani 1 1 d .
H28 H 0.0632 0.0560 0.9053 0.041 Uiso 1 1 d R
C29 C -0.1372(10) 0.03674(17) 0.8252(8) 0.0423(18) Uani 1 1 d .
H29 H -0.0980 0.0177 0.7952 0.051 Uiso 1 1 d R
C30 C -0.2878(10) 0.0418(2) 0.8039(8) 0.046(2) Uani 1 1 d .
H30 H -0.3537 0.0260 0.7610 0.055 Uiso 1 1 d R
C31 C -0.3444(9) 0.0689(2) 0.8448(8) 0.0396(17) Uani 1 1 d .
H31 H -0.4490 0.0723 0.8284 0.048 Uiso 1 1 d R
C32 C -0.2498(8) 0.09182(17) 0.9107(7) 0.0335(15) Uani 1 1 d .
H32 H -0.2916 0.1108 0.9387 0.040 Uiso 1 1 d R
C33 C -0.0741(7) 0.13178(15) 1.1452(6) 0.0259(12) Uani 1 1 d .
C34 C -0.0682(9) 0.16306(16) 1.1907(7) 0.0346(15) Uani 1 1 d .
H34 H -0.0080 0.1790 1.1629 0.042 Uiso 1 1 d R
C35 C -0.1480(10) 0.17143(18) 1.2782(8) 0.0416(18) Uani 1 1 d .
H35 H -0.1436 0.1930 1.3089 0.050 Uiso 1 1 d R
C36 C -0.2338(9) 0.14833(18) 1.3204(8) 0.0390(17) Uani 1 1 d .
H36 H -0.2915 0.1545 1.3777 0.047 Uiso 1 1 d R
C37 C -0.2349(8) 0.11707(18) 1.2781(7) 0.0351(15) Uani 1 1 d .
H37 H -0.2909 0.1008 1.3085 0.042 Uiso 1 1 d R
C38 C -0.1559(7) 0.10898(16) 1.1922(7) 0.0317(14) Uani 1 1 d .
H38 H -0.1580 0.0871 1.1651 0.038 Uiso 1 1 d R
C39 C 0.1931(9) 0.05370(16) 1.1871(7) 0.0349(15) Uani 1 1 d .
H39A H 0.2804 0.0433 1.2305 0.042 Uiso 1 1 d R
H39B H 0.1475 0.0403 1.1215 0.042 Uiso 1 1 d R
H39C H 0.1255 0.0572 1.2394 0.042 Uiso 1 1 d R
C40 C 0.3927(9) 0.0860(2) 1.0406(8) 0.0419(18) Uani 1 1 d .
H40A H 0.4742 0.0756 1.0917 0.050 Uiso 1 1 d R
H40B H 0.4251 0.1060 1.0128 0.050 Uiso 1 1 d R
H40C H 0.3548 0.0724 0.9734 0.050 Uiso 1 1 d R
C41 C 0.3245(8) 0.12085(17) 1.2562(8) 0.0375(16) Uani 1 1 d .
H41A H 0.4120 0.1112 1.3023 0.045 Uiso 1 1 d R
H41B H 0.2534 0.1238 1.3059 0.045 Uiso 1 1 d R
H41C H 0.3486 0.1413 1.2263 0.045 Uiso 1 1 d R
C42 C 0.7392(9) 0.01999(16) 0.2435(8) 0.0354(15) Uani 1 1 d .
C43 C 0.8574(9) 0.02337(18) 0.3383(9) 0.0438(19) Uani 1 1 d .
H43 H 0.9565 0.0219 0.3255 0.053 Uiso 1 1 d R
C44 C 0.8360(9) 0.02885(18) 0.4558(9) 0.0429(19) Uani 1 1 d .
H44 H 0.9194 0.0317 0.5203 0.052 Uiso 1 1 d R
C45 C 0.6956(10) 0.03018(19) 0.4788(8) 0.0440(18) Uani 1 1 d .
H45 H 0.6828 0.0341 0.5590 0.053 Uiso 1 1 d R
C46 C 0.5752(11) 0.0261(2) 0.3845(9) 0.050(2) Uani 1 1 d .
H46 H 0.4766 0.0264 0.3990 0.060 Uiso 1 1 d R
C47 C 0.5976(9) 0.02135(19) 0.2683(9) 0.0427(19) Uani 1 1 d .
H47 H 0.5127 0.0190 0.2048 0.051 Uiso 1 1 d R
C48 C 0.7577(13) 0.0144(2) 0.1202(9) 0.053(2) Uani 1 1 d .
H48A H 0.6621 0.0128 0.0687 0.064 Uiso 1 1 d R
H48B H 0.8117 -0.0051 0.1160 0.064 Uiso 1 1 d R
H48C H 0.8103 0.0322 0.0950 0.064 Uiso 1 1 d R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
P2 Pt1 P1 85.92(6)
P2 Pt1 Si1 101.19(6)
P1 Pt1 Si1 172.85(6)
P2 Pt1 H1 177(3)
P1 Pt1 H1 91(3)
Si1 Pt1 H1 82(3)
C3 P1 C9 103.4(3)
C3 P1 C1 104.7(4)
C9 P1 C1 106.0(3)
C3 P1 Pt1 120.3(3)
C9 P1 Pt1 113.3(2)
C1 P1 Pt1 108.1(2)
C21 P2 C15 105.5(3)
C21 P2 C2 101.1(3)
C15 P2 C2 104.5(3)
C21 P2 Pt1 119.8(3)
C15 P2 Pt1 116.6(2)
C2 P2 Pt1 107.3(2)
C27 Si1 C33 102.4(3)
C27 Si1 Si2 108.2(2)
C33 Si1 Si2 103.20(19)
C27 Si1 Pt1 117.9(2)
C33 Si1 Pt1 115.9(2)
Si2 Si1 Pt1 108.16(8)
C41 Si2 C40 107.0(4)
C41 Si2 C39 109.5(4)
C40 Si2 C39 107.4(4)
C41 Si2 Si1 106.9(2)
C40 Si2 Si1 115.6(3)
C39 Si2 Si1 110.1(2)
C2 C1 P1 109.8(5)
C2 C1 H1A 109.6
P1 C1 H1A 109.6
C2 C1 H1B 109.0
P1 C1 H1B 109.3
H1A C1 H1B 109.5
C1 C2 P2 109.6(5)
C1 C2 H2A 109.3
P2 C2 H2A 109.2
C1 C2 H2B 109.8
P2 C2 H2B 109.5
H2A C2 H2B 109.5
C8 C3 C4 119.7(7)
C8 C3 P1 119.9(6)
C4 C3 P1 120.3(6)
C5 C4 C3 120.3(8)
C5 C4 H4 119.7
C3 C4 H4 120.1
C4 C5 C6 119.4(9)
C4 C5 H5 119.6
C6 C5 H5 121.0
C7 C6 C5 120.9(8)
C7 C6 H6 119.4
C5 C6 H6 119.7
C6 C7 C8 121.5(9)
C6 C7 H7 120.2
C8 C7 H7 118.2
C3 C8 C7 118.2(9)
C3 C8 H8 119.7
C7 C8 H8 122.1
C14 C9 C10 118.5(7)
C14 C9 P1 117.4(5)
C10 C9 P1 124.1(6)
C11 C10 C9 120.3(8)
C11 C10 H10 120.0
C9 C10 H10 119.6
C12 C11 C10 120.4(7)
C12 C11 H11 119.3
C10 C11 H11 120.3
C11 C12 C13 120.3(7)
C11 C12 H12 120.1
C13 C12 H12 119.7
C14 C13 C12 118.8(8)
C14 C13 H13 121.5
C12 C13 H13 119.8
C13 C14 C9 121.7(7)
C13 C14 H14 118.4
C9 C14 H14 119.9
C20 C15 C16 119.9(6)
C20 C15 P2 123.0(5)
C16 C15 P2 117.2(6)
C17 C16 C15 119.5(7)
C17 C16 H16 120.5
C15 C16 H16 120.0
C16 C17 C18 120.9(7)
C16 C17 H17 120.2
C18 C17 H17 118.9
C19 C18 C17 119.0(7)
C19 C18 H18 121.2
C17 C18 H18 119.8
C18 C19 C20 120.4(8)
C18 C19 H19 119.6
C20 C19 H19 120.0
C15 C20 C19 120.3(7)
C15 C20 H20 119.7
C19 C20 H20 120.1
C22 C21 C26 119.7(6)
C22 C21 P2 124.6(5)
C26 C21 P2 115.6(5)
C21 C22 C23 119.5(6)
C21 C22 H22 119.8
C23 C22 H22 120.8
C24 C23 C22 120.9(6)
C24 C23 H23 119.1
C22 C23 H23 120.0
C23 C24 C25 120.0(6)
C23 C24 H24 120.1
C25 C24 H24 119.9
C24 C25 C26 120.3(7)
C24 C25 H25 120.1
C26 C25 H25 119.6
C25 C26 C21 119.6(6)
C25 C26 H26 120.7
C21 C26 H26 119.7
C32 C27 C28 117.4(6)
C32 C27 Si1 120.5(5)
C28 C27 Si1 122.1(5)
C29 C28 C27 120.8(7)
C29 C28 H28 119.9
C27 C28 H28 119.4
C30 C29 C28 119.9(8)
C30 C29 H29 120.2
C28 C29 H29 120.0
C31 C30 C29 120.5(7)
C31 C30 H30 119.4
C29 C30 H30 120.1
C30 C31 C32 120.2(8)
C30 C31 H31 119.8
C32 C31 H31 120.0
C27 C32 C31 121.2(7)
C27 C32 H32 119.8
C31 C32 H32 119.0
C38 C33 C34 118.4(7)
C38 C33 Si1 119.7(5)
C34 C33 Si1 121.9(6)
C33 C34 C35 120.6(7)
C33 C34 H34 120.0
C35 C34 H34 119.3
C36 C35 C34 119.7(7)
C36 C35 H35 120.2
C34 C35 H35 120.2
C37 C36 C35 119.4(9)
C37 C36 H36 121.4
C35 C36 H36 119.2
C38 C37 C36 120.6(8)
C38 C37 H37 119.2
C36 C37 H37 120.2
C37 C38 C33 121.2(7)
C37 C38 H38 118.7
C33 C38 H38 120.0
Si2 C39 H39A 109.7
Si2 C39 H39B 109.4
H39A C39 H39B 109.5
Si2 C39 H39C 109.3
H39A C39 H39C 109.5
H39B C39 H39C 109.5
Si2 C40 H40A 109.1
Si2 C40 H40B 109.8
H40A C40 H40B 109.5
Si2 C40 H40C 109.4
H40A C40 H40C 109.5
H40B C40 H40C 109.5
Si2 C41 H41A 109.7
Si2 C41 H41B 109.0
H41A C41 H41B 109.5
Si2 C41 H41C 109.7
H41A C41 H41C 109.5
H41B C41 H41C 109.5
C43 C42 C47 117.6(9)
C43 C42 C48 122.6(9)
C47 C42 C48 119.7(8)
C42 C43 C44 121.3(8)
C42 C43 H43 120.3
C44 C43 H43 118.5
C45 C44 C43 120.4(7)
C45 C44 H44 119.5
C43 C44 H44 120.1
C44 C45 C46 119.0(9)
C44 C45 H45 119.4
C46 C45 H45 121.5
C45 C46 C47 120.1(9)
C45 C46 H46 120.3
C47 C46 H46 119.6
C42 C47 C46 121.6(8)
C42 C47 H47 120.1
C46 C47 H47 118.4
C42 C48 H48A 109.0
C42 C48 H48B 110.1
H48A C48 H48B 109.5
C42 C48 H48C 109.3
H48A C48 H48C 109.5
H48B C48 H48C 109.5
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Pt1 P2 2.2877(16)
Pt1 P1 2.3000(17)
Pt1 Si1 2.3694(18)
Pt1 H1 1.49(9)
P1 C3 1.820(7)
P1 C9 1.825(7)
P1 C1 1.838(8)
P2 C21 1.817(7)
P2 C15 1.829(7)
P2 C2 1.855(7)
Si1 C27 1.905(7)
Si1 C33 1.936(8)
Si1 Si2 2.362(2)
Si2 C41 1.882(8)
Si2 C40 1.886(10)
Si2 C39 1.890(7)
C1 C2 1.540(9)
C1 H1A 0.9601
C1 H1B 0.9599
C2 H2A 0.9600
C2 H2B 0.9601
C3 C8 1.392(11)
C3 C4 1.419(11)
C4 C5 1.391(10)
C4 H4 0.9600
C5 C6 1.391(16)
C5 H5 0.9599
C6 C7 1.350(17)
C6 H6 0.9600
C7 C8 1.424(12)
C7 H7 0.9600
C8 H8 0.9599
C9 C14 1.398(11)
C9 C10 1.405(9)
C10 C11 1.388(11)
C10 H10 0.9600
C11 C12 1.385(13)
C11 H11 0.9601
C12 C13 1.410(12)
C12 H12 0.9600
C13 C14 1.383(11)
C13 H13 0.9600
C14 H14 0.9600
C15 C20 1.382(10)
C15 C16 1.413(9)
C16 C17 1.384(10)
C16 H16 0.9599
C17 C18 1.405(13)
C17 H17 0.9601
C18 C19 1.394(12)
C18 H18 0.9600
C19 C20 1.399(11)
C19 H19 0.9600
C20 H20 0.9602
C21 C22 1.387(9)
C21 C26 1.402(10)
C22 C23 1.401(9)
C22 H22 0.9600
C23 C24 1.367(10)
C23 H23 0.9599
C24 C25 1.383(10)
C24 H24 0.9600
C25 C26 1.397(10)
C25 H25 0.9601
C26 H26 0.9600
C27 C32 1.397(9)
C27 C28 1.412(10)
C28 C29 1.403(10)
C28 H28 0.9600
C29 C30 1.383(13)
C29 H29 0.9600
C30 C31 1.366(14)
C30 H30 0.9601
C31 C32 1.404(10)
C31 H31 0.9600
C32 H32 0.9599
C33 C38 1.387(10)
C33 C34 1.397(9)
C34 C35 1.402(12)
C34 H34 0.9600
C35 C36 1.392(14)
C35 H35 0.9603
C36 C37 1.385(11)
C36 H36 0.9599
C37 C38 1.379(11)
C37 H37 0.9600
C38 H38 0.9599
C39 H39A 0.9600
C39 H39B 0.9598
C39 H39C 0.9599
C40 H40A 0.9599
C40 H40B 0.9599
C40 H40C 0.9602
C41 H41A 0.9600
C41 H41B 0.9600
C41 H41C 0.9598
C42 C43 1.382(12)
C42 C47 1.398(12)
C42 C48 1.471(13)
C43 C44 1.414(14)
C43 H43 0.9599
C44 C45 1.379(13)
C44 H44 0.9600
C45 C46 1.395(12)
C45 H45 0.9600
C46 C47 1.398(14)
C46 H46 0.9599
C47 H47 0.9600
C48 H48A 0.9600
C48 H48B 0.9597
C48 H48C 0.9602
