Crystallography Open Database

Information card for entry 7025466

Preview

Coordinates	7025466.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H44 Cl4 N12 O16 Pt
Calculated formula	C26 H44 Cl4 N12 O16 Pt
SMILES	C(CNC(CC)=[NH][Pt]([NH]=C(CC)NCC[NH3+])(Cl)(Cl)(Cl)Cl)[NH3+].c1([O-])c(cc(cc1N(=O)=O)N(=O)=O)N(=O)=O.OCC.c1([O-])c(cc(N(=O)=O)cc1N(=O)=O)N(=O)=O.OCC
Title of publication	One-end nucleophilic addition of di- and triamines to Pt(IV)-coordinated nitriles as an entry to (amidine)Pt(IV) complexes bearing pendant NH₂-groups.
Authors of publication	Bokach, Nadezhda A.; Konovalova, Nina P.; Wang, Yu; Moskalenko, Yulia E.; Gribanov, Alexander V.; Kukushkin, Vadim Yu
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	19
Pages of publication	4619 - 4623
a	8.9708 ± 0.0006 Å
b	11.559 ± 0.0007 Å
c	11.5958 ± 0.0007 Å
α	61.723 ± 0.001°
β	80.464 ± 0.001°
γ	78.18 ± 0.001°
Cell volume	1033.18 ± 0.11 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0266
Residual factor for significantly intense reflections	0.0266
Weighted residual factors for significantly intense reflections	0.064
Weighted residual factors for all reflections included in the refinement	0.064
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179960 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/54.	7025466.cif
130086	2015-01-23	cod/ (robertas@burundukas) The 'cif_fix_values' program was applied to CIFs that have generated the validation messages containing tag '_exptl_crystal_density_meas'. 16946 CIFs had a values that were perceived as 'not measured' and they were changed to '?'. The total of 17089 CIFs was changed. Those that were not corrected by 'cif_fix_values' were reformatted by the parser (e.g. a doi tag was moved to another place). The processing command was: mysql -u cod_reader -h www.crystallography.net cod -e \ 'select distinct codid from validation \ where message like \ "%tag%_exptl_crystal_density_meas'\''%"' -NB \ \| xargs -i sh -c 'cif_fix_values {} \ \| cif_filter --add-cif-header {} \ \| sponge {}'	7025466.cif
93063	2014-01-12	cif/ Adding structures of 7025466 via cif-deposit CGI script.	7025466.cif