Crystallography Open Database

Information card for entry 7025987

Preview

Coordinates	7025987.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	1,2-bis(tris(trimethylsilyl)methyl)disilane
Formula	C20 H58 Si8
Calculated formula	C20 H58 Si8
Title of publication	The gas-phase structure and some reactions of the bulky primary silane (Me(3)Si)(3)CSiH(3) and the solid-state structure of the bulky dialkyl disilane [(Me(3)Si)(3)CSiH(2)](2).
Authors of publication	Masters, Sarah L.; Rankin, David W. H.; Cordes, David B.; Bätz, Karin; Lickiss, Paul D.; Boag, Neil M.; Redhouse, Alan D.; Whittaker, Stephen M.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	39
Pages of publication	9353 - 9360
a	9.09 ± 0.004 Å
b	12.712 ± 0.004 Å
c	15.286 ± 0.005 Å
α	108.29 ± 0.03°
β	90.32 ± 0.03°
γ	91.49 ± 0.03°
Cell volume	1676.4 ± 1.1 Å³
Cell temperature	203 ± 2 K
Ambient diffraction temperature	203 ± 2 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0649
Residual factor for significantly intense reflections	0.0455
Weighted residual factors for significantly intense reflections	0.1044
Weighted residual factors for all reflections included in the refinement	0.1121
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179965 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/59.	7025987.cif
93372	2014-01-13	cif/ Adding structures of 7025987 via cif-deposit CGI script.	7025987.cif