Crystallography Open Database

Information card for entry 7026033

Preview

Coordinates	7026033.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C57.5 H78 N6 O5 Si Zn
Calculated formula	C57.5 H78 N6 O5 Si Zn
Title of publication	Coordination of a Si[double bond, length as m-dash]O subunit to metals: complexes of donor-stabilized silanone featuring a terminal Si[double bond, length as m-dash]O→M coordination (M = Zn, Al).
Authors of publication	Xiong, Yun; Yao, Shenglai; Driess, Matthias
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	39
Pages of publication	9282 - 9287
a	14.5359 ± 0.0004 Å
b	21.7258 ± 0.0005 Å
c	17.8232 ± 0.0004 Å
α	90°
β	90.067 ± 0.002°
γ	90°
Cell volume	5628.6 ± 0.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0865
Residual factor for significantly intense reflections	0.0485
Weighted residual factors for significantly intense reflections	0.1053
Weighted residual factors for all reflections included in the refinement	0.1144
Goodness-of-fit parameter for all reflections included in the refinement	0.973
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7026033.cif
93390	2014-01-13	cif/ Adding structures of 7026033, 7026034, 7026035, 7026036 via cif-deposit CGI script.	7026033.cif