Crystallography Open Database

Information card for entry 7026036

Preview

Coordinates	7026036.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C53 H75 Al N4 O Si
Calculated formula	C53 H75 Al N4 O Si
Title of publication	Coordination of a Si[double bond, length as m-dash]O subunit to metals: complexes of donor-stabilized silanone featuring a terminal Si[double bond, length as m-dash]O→M coordination (M = Zn, Al).
Authors of publication	Xiong, Yun; Yao, Shenglai; Driess, Matthias
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	39
Pages of publication	9282 - 9287
a	11.3598 ± 0.0003 Å
b	14.2375 ± 0.0006 Å
c	17.696 ± 0.0009 Å
α	108.081 ± 0.004°
β	98.036 ± 0.003°
γ	90.78 ± 0.003°
Cell volume	2689.1 ± 0.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1165
Residual factor for significantly intense reflections	0.0704
Weighted residual factors for significantly intense reflections	0.1586
Weighted residual factors for all reflections included in the refinement	0.1762
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179966 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/60.	7026036.cif
93390	2014-01-13	cif/ Adding structures of 7026033, 7026034, 7026035, 7026036 via cif-deposit CGI script.	7026036.cif