Crystallography Open Database

Information card for entry 7026401

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Coordinates	7026401.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H38 N6 Si
Calculated formula	C28 H38 N6 Si
SMILES	C(#N)[Si]12(C#N)([N](C(C)C)=C(c3ccccc3)N2C(C)C)[N](C(C)C)=C(c2ccccc2)N1C(C)C
Title of publication	Novel neutral hexacoordinate silicon(IV) complexes with two bidentate monoanionic benzamidinato ligands.
Authors of publication	Junold, Konstantin; Burschka, Christian; Bertermann, Rüdiger; Tacke, Reinhold
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	39
Pages of publication	9401 - 9413
a	9.688 ± 0.0019 Å
b	18.094 ± 0.004 Å
c	16.31 ± 0.003 Å
α	90°
β	95.4 ± 0.03°
γ	90°
Cell volume	2846.4 ± 1 Å³
Cell temperature	183 ± 2 K
Ambient diffraction temperature	183 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0656
Residual factor for significantly intense reflections	0.0411
Weighted residual factors for significantly intense reflections	0.1002
Weighted residual factors for all reflections included in the refinement	0.1081
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179970 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/64.	7026401.cif
93489	2014-01-13	cif/ Adding structures of 7026399, 7026400, 7026401, 7026402, 7026403, 7026404, 7026405, 7026406, 7026407 via cif-deposit CGI script.	7026401.cif