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Information card for entry 7027050
Preview
| Coordinates | 7027050.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C42 H59 B N5 O4 Tc |
|---|---|
| Calculated formula | C42 H59 B N5 O4 Tc |
| Title of publication | Crystal structures of nitridotechnetium(V) complexes of amine oximes differing in carbon chain lengths |
| Authors of publication | Kani, Yuko; TakayamaTsutomuSekine, Tsutomu; Kudo, Hiroshi |
| Journal of publication | Journal of the Chemical Society, Dalton Transactions |
| Year of publication | 1999 |
| Journal issue | 2 |
| Pages of publication | 209 |
| a | 9.986 ± 0.005 Å |
| b | 30.636 ± 0.002 Å |
| c | 13.967 ± 0.003 Å |
| α | 90° |
| β | 95.24 ± 0.03° |
| γ | 90° |
| Cell volume | 4255 ± 2 Å3 |
| Cell temperature | 286.2 K |
| Ambient diffraction temperature | 286.2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for significantly intense reflections | 0.0337 |
| Weighted residual factors for significantly intense reflections | 0.036 |
| Goodness-of-fit parameter for significantly intense reflections | 1.3 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176453 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7. |
7027050.cif |
| 130086 | 2015-01-23 | cod/ (robertas@burundukas) The 'cif_fix_values' program was applied to CIFs that have generated the validation messages containing tag '_exptl_crystal_density_meas'. 16946 CIFs had a values that were perceived as 'not measured' and they were changed to '?'. The total of 17089 CIFs was changed. Those that were not corrected by 'cif_fix_values' were reformatted by the parser (e.g. a doi tag was moved to another place). The processing command was: mysql -u cod_reader -h www.crystallography.net cod -e \ 'select distinct codid from validation \ where message like \ "%tag%_exptl_crystal_density_meas'\''%"' -NB \ | xargs -i sh -c 'cif_fix_values {} \ | cif_filter --add-cif-header {} \ | sponge {}' |
7027050.cif |
| 94946 | 2014-01-28 | cif/ Adding structures of 7027049, 7027050 via cif-deposit CGI script. |
7027050.cif |
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Users of the data should acknowledge the original authors of the
structural data.