Crystallography Open Database

Information card for entry 7027432

Preview

Coordinates	7027432.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H22 As Li O2
Calculated formula	C14 H21 As Li O2
Title of publication	A metallated primary arsine; synthesis and structure of [PhAsHLi·2thf ]\ιnfty
Authors of publication	Beswick, Michael A.; Lawson, Yvonne G.; Raithby, Paul R.; Wood, Jody A.; Wright, Dominic S.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	12
Pages of publication	1921
a	8.15 ± 0.002 Å
b	8.564 ± 0.002 Å
c	11.278 ± 0.002 Å
α	90°
β	101.87 ± 0.03°
γ	90°
Cell volume	770.3 ± 0.3 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.1293
Residual factor for significantly intense reflections	0.104
Weighted residual factors for significantly intense reflections	0.2339
Weighted residual factors for all reflections included in the refinement	0.2439
Goodness-of-fit parameter for all reflections included in the refinement	1.595
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179980 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/74.	7027432.cif
95372	2014-01-28	cif/ Adding structures of 7027432 via cif-deposit CGI script.	7027432.cif