Crystallography Open Database

Information card for entry 7027441

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Coordinates	7027441.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H40 O2 Sb2 Si2
Calculated formula	C26 H40 O2 Sb2 Si2
SMILES	O(C(=[Sb][Sb]=C(c1c(cc(cc1C)C)C)O[Si](C)(C)C)c1c(cc(cc1C)C)C)[Si](C)(C)C
Title of publication	Compounds containing λ3,σ2-SbC bonds: synthesis and structural characterisation of the first stiba-enol, MesC(O)SbC(OH)Mes (Mes* = C6H2But3-2,4,6) and a 2,3-distibabutadiene, {Mes(Me3SiO)CSb}2 (Mes = C6H2Me3-2,4,6) †
Authors of publication	Jones, Cameron; Steed, Jonathan W.; Thomas, Ryan C.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	10
Pages of publication	1541
a	10.704 ± 0.002 Å
b	14.043 ± 0.003 Å
c	10.889 ± 0.002 Å
α	90°
β	109.57 ± 0.03°
γ	90°
Cell volume	1542.2 ± 0.6 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0482
Residual factor for significantly intense reflections	0.0331
Weighted residual factors for significantly intense reflections	0.094
Weighted residual factors for all reflections included in the refinement	0.1127
Goodness-of-fit parameter for all reflections included in the refinement	0.502
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179980 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/74.	7027441.cif
95380	2014-01-28	cif/ Adding structures of 7027441, 7027442 via cif-deposit CGI script.	7027441.cif