Crystallography Open Database

Information card for entry 7027469

Preview

Coordinates	7027469.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H40 O5 Os
Calculated formula	C24 H31.2 O5 Os
Title of publication	Preparation and crystal structures of oxoosmium(VI) diolato complexes
Authors of publication	Lehtonen, Ari; Jokela, Jukka; Edwards, Peter G.; Sillanpää, Reijo
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	16
Pages of publication	2785 - 2788
a	16.421 ± 0.008 Å
b	17.103 ± 0.005 Å
c	12.299 ± 0.005 Å
α	107.61 ± 0.03°
β	96.28 ± 0.04°
γ	67.01 ± 0.03°
Cell volume	3031 ± 2 Å³
Cell temperature	294 ± 2 K
Ambient diffraction temperature	294 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0938
Residual factor for significantly intense reflections	0.0433
Weighted residual factors for significantly intense reflections	0.0882
Weighted residual factors for all reflections included in the refinement	0.0996
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
134365 (current)	2015-03-25	cif/7/02/74/ (antanas@echidna.ibt.lt) Changing the '_atom_site_refinement_flags' tag value for atom 'H32A' from 'Z' to 'R' after consulting the original paper for CIF 7027469.	7027469.cif
95402	2014-01-28	cif/ Adding structures of 7027467, 7027468, 7027469 via cif-deposit CGI script.	7027469.cif