Crystallography Open Database

Information card for entry 7027785

Preview

Coordinates	7027785.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H60 Cl2 Mg2 O2 P2
Calculated formula	C30 H60 Cl2 Mg2 O2 P2
Title of publication	A convenient synthetic route to substituted phosphavinyl Grignard reagents: synthesis and characterisation of [{RPC(But)MgX(OEt2)}2] (R = cyclohexyl, cyclopentyl, ethyl or mesityl; X = Cl or Br) †
Authors of publication	Hibbs, David E.; Jones, Cameron; Richards, Anne F.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	20
Pages of publication	3531
a	11.6149 ± 0.0005 Å
b	12.441 ± 0.0007 Å
c	15.8853 ± 0.0004 Å
α	72.073 ± 0.003°
β	70.757 ± 0.003°
γ	65.849 ± 0.003°
Cell volume	1937.23 ± 0.16 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0995
Residual factor for significantly intense reflections	0.0545
Weighted residual factors for significantly intense reflections	0.1299
Weighted residual factors for all reflections included in the refinement	0.1462
Goodness-of-fit parameter for all reflections included in the refinement	0.991
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179983 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/77.	7027785.cif
95785	2014-01-28	cif/ Adding structures of 7027785, 7027786 via cif-deposit CGI script.	7027785.cif