Crystallography Open Database

Information card for entry 7028804

Preview

Coordinates	7028804.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H68 Dy Li N8 Si4
Calculated formula	C44 H68 Dy Li N8 Si4
Title of publication	Synthesis, structure, and catalytic activity of novel trinuclear rare-earth metal amido complexes incorporating μ-η(5):η(1) bonding indolyl and μ3-oxo groups.
Authors of publication	Yang, Song; Zhu, Xiancui; Zhou, Shuangliu; Wang, Shaowu; Feng, Zhijun; Wei, Yun; Miao, Hui; Guo, Liping; Wang, Fenhua; Zhang, Guangchao; Gu, Xiaoxia; Mu, Xiaolong
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	6
Pages of publication	2521 - 2533
a	13.4676 ± 0.0013 Å
b	17.2921 ± 0.0017 Å
c	45.497 ± 0.004 Å
α	90°
β	95.663 ± 0.001°
γ	90°
Cell volume	10543.8 ± 1.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1515
Residual factor for significantly intense reflections	0.0687
Weighted residual factors for significantly intense reflections	0.1592
Weighted residual factors for all reflections included in the refinement	0.1877
Goodness-of-fit parameter for all reflections included in the refinement	0.94
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179994 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/88.	7028804.cif
105429	2014-03-12	cif/ Adding structures of 7028798, 7028799, 7028800, 7028801, 7028802, 7028803, 7028804 via cif-deposit CGI script.	7028804.cif