Crystallography Open Database

Information card for entry 7029044

Preview

Coordinates	7029044.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C96 H106 N12 O22 P4 Sn6
Calculated formula	C96 H106 N12 O22 P4 Sn6
Title of publication	Assembly of hexa- and trinuclear monoorganostannoxanes: hemi-labile nature of intramolecular N→Sn coordination in RSnCl3 (R = 2-phenylazophenyl).
Authors of publication	Metre, Ramesh K.; Mohapatra, Chandrajeet; Sahoo, Dipankar; Chandrasekhar, Vadapalli
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	8
Pages of publication	3364 - 3371
a	15.686 ± 0.005 Å
b	16.555 ± 0.005 Å
c	25.329 ± 0.005 Å
α	94.871 ± 0.005°
β	104.68 ± 0.005°
γ	109.436 ± 0.005°
Cell volume	5896 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0988
Residual factor for significantly intense reflections	0.0658
Weighted residual factors for significantly intense reflections	0.1658
Weighted residual factors for all reflections included in the refinement	0.1914
Goodness-of-fit parameter for all reflections included in the refinement	0.956
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179996 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/90.	7029044.cif
105493	2014-03-12	cif/ Adding structures of 7029044, 7029045, 7029046, 7029047, 7029048 via cif-deposit CGI script.	7029044.cif