Crystallography Open Database

Information card for entry 7029126

Preview

Coordinates	7029126.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C72 H77 Cl9 O4 P3 Rh
Calculated formula	C72 H75 Cl9 O4 P3 Rh
Title of publication	Mixed anhydride complexes of rhodium(i) and ruthenium(ii) - their synthesis and ligand rearrangements.
Authors of publication	Coetzee, Jacorien; Eastham, Graham R.; Slawin, Alexandra M. Z.; Cole-Hamilton, David J
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	9
Pages of publication	3479 - 3491
a	12.273 ± 0.004 Å
b	14.006 ± 0.003 Å
c	20.777 ± 0.006 Å
α	93.707 ± 0.008°
β	91.581 ± 0.006°
γ	93.876 ± 0.01°
Cell volume	3554 ± 1.7 Å³
Cell temperature	93 K
Ambient diffraction temperature	93 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0971
Weighted residual factors for all reflections included in the refinement	0.2744
Goodness-of-fit parameter for all reflections included in the refinement	0.956
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179997 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/91.	7029126.cif
105518	2014-03-12	cif/ Adding structures of 7029122, 7029123, 7029124, 7029125, 7029126 via cif-deposit CGI script.	7029126.cif