Crystallography Open Database

Information card for entry 7029361

Preview

Coordinates	7029361.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C51 H87 N5 Si2 Yb
Calculated formula	C51 H80 N5 Si2 Yb
Title of publication	Synthesis of γ-amidine-functionalized dianionic β-diketiminato lanthanide amides and trianionic β-diketiminato Na/Sm heterobimetallic complexes and their reactivity in polymerization of l-lactide.
Authors of publication	Liu, Peng; Chen, Hongxia; Zhang, Yong; Xue, Mingqiang; Yao, Yingming; Shen, Qi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	14
Pages of publication	5586 - 5594
a	11.4354 ± 0.0003 Å
b	12.4814 ± 0.0003 Å
c	19.2857 ± 0.0005 Å
α	99.15 ± 0.002°
β	101.425 ± 0.002°
γ	92.695 ± 0.002°
Cell volume	2654.98 ± 0.12 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0416
Residual factor for significantly intense reflections	0.0374
Weighted residual factors for significantly intense reflections	0.0878
Weighted residual factors for all reflections included in the refinement	0.0904
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179999 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/93.	7029361.cif
107133	2014-03-18	cif/ Adding structures of 7029360, 7029361, 7029362, 7029363, 7029364 via cif-deposit CGI script.	7029361.cif