Crystallography Open Database

Information card for entry 7029705

Preview

Coordinates	7029705.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C75 H114 Li2 N5 Nd O2
Calculated formula	C75 H114 Li2 N5 Nd O2
Title of publication	Lanthanide anilido complexes: synthesis, characterization, and use as highly efficient catalysts for hydrophosphonylation of aldehydes and unactivated ketones.
Authors of publication	Liu, Chengwei; Qian, Qinqin; Nie, Kun; Wang, Yaorong; Shen, Qi; Yuan, Dan; Yao, Yingming
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	22
Pages of publication	8355 - 8362
a	22.608 ± 0.005 Å
b	13.933 ± 0.003 Å
c	23.885 ± 0.006 Å
α	90°
β	104.512 ± 0.005°
γ	90°
Cell volume	7284 ± 3 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1542
Residual factor for significantly intense reflections	0.1026
Weighted residual factors for significantly intense reflections	0.2371
Weighted residual factors for all reflections included in the refinement	0.2899
Goodness-of-fit parameter for all reflections included in the refinement	1.142
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180003 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/97.	7029705.cif
116206	2014-06-07	cif/ Updating files of 7029704, 7029705, 7029706 Original log message: Adding full bibliography for 7029704--7029706.cif.	7029705.cif
109500	2014-04-15	cif/ Adding structures of 7029704, 7029705, 7029706 via cif-deposit CGI script.	7029705.cif