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Information card for entry 7029728
Preview
| Coordinates | 7029728.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C48 H69 Lu N P Si2 |
|---|---|
| Calculated formula | C48 H69 Lu N P Si2 |
| SMILES | [c]123[cH]4[c]56[c]7(C(CC5(C)C)(C)C)[cH]1[Lu]3467(C[Si](C)(C)C)(C[Si](C)(C)C)[N](C13CC4CC(CC(C3)C4)C1)=P2(c1ccccc1)c1ccccc1.c1ccccc1 |
| Title of publication | Tetrahydropentalenyl-phosphazene constrained geometry complexes of rare-earth metal alkyls. |
| Authors of publication | Hangaly, Noa K; Petrov, Alexander R; Elfferding, Michael; Harms, Klaus; Sundermeyer, Jörg |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2014 |
| Journal volume | 43 |
| Journal issue | 19 |
| Pages of publication | 7109 - 7120 |
| a | 10.8236 ± 0.0008 Å |
| b | 12.8149 ± 0.0009 Å |
| c | 17.0962 ± 0.0013 Å |
| α | 93.599 ± 0.009° |
| β | 103.167 ± 0.008° |
| γ | 91.998 ± 0.008° |
| Cell volume | 2301.5 ± 0.3 Å3 |
| Cell temperature | 193 ± 2 K |
| Ambient diffraction temperature | 193 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0233 |
| Residual factor for significantly intense reflections | 0.0177 |
| Weighted residual factors for significantly intense reflections | 0.0351 |
| Weighted residual factors for all reflections included in the refinement | 0.0356 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.909 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 180003 (current) | 2016-03-25 | cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/97. |
7029728.cif |
| 111192 | 2014-04-21 | cif/ Updating files of 7029728 Original log message: Adding full bibliography for ./tmp-cod-update-bibliographies-12899/cifs/7029728.cif. |
7029728.cif |
| 109539 | 2014-04-16 | cif/ Adding structures of 7029725, 7029726, 7029727, 7029728, 7029729, 7029730, 7029731 via cif-deposit CGI script. |
7029728.cif |
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Users of the data should acknowledge the original authors of the
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