Crystallography Open Database

Information card for entry 7030109

Preview

Coordinates	7030109.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H44 Li N5 O
Calculated formula	C21.988 H44 Li N5 O
Title of publication	Lithium, sodium and potassium picolyl complexes: syntheses, structures and bonding.
Authors of publication	Kennedy, Alan R.; Mulvey, Robert E.; Urquhart, Robert I.; Robertson, Stuart D.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	38
Pages of publication	14265 - 14274
a	9.39 ± 0.0003 Å
b	14.715 ± 0.0004 Å
c	18.0296 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	2491.22 ± 0.12 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	5
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0786
Residual factor for significantly intense reflections	0.0588
Weighted residual factors for significantly intense reflections	0.135
Weighted residual factors for all reflections included in the refinement	0.1458
Goodness-of-fit parameter for all reflections included in the refinement	1.073
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180007 (current)	2016-03-25	cif/7/03/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/03/01.	7030109.cif
124728	2014-10-06	cif/ Updating files of 7030109, 7030110, 7030111, 7030112, 7030113, 7030114 Original log message: Adding full bibliography for 7030109--7030114.cif.	7030109.cif
111468	2014-04-23	cif/ Adding structures of 7030109, 7030110, 7030111, 7030112, 7030113, 7030114 via cif-deposit CGI script.	7030109.cif