Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7031299
Preview
| Coordinates | 7031299.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | moris347 |
|---|---|
| Formula | C37 H55 Cl3 N6 Si2 U |
| Calculated formula | C37 H55 Cl3 N6 Si2 U |
| SMILES | [U]123(Cl)(Cl)[N](C(C)(C)C)=C(N1[Si](N(C(C)(C)C)C(=[N]2[Si]([N]3=C(NC(C)(C)C)c1ccccc1)(C)C)c1ccccc1)(C)C)c1ccccc1.[Cl-] |
| Title of publication | Dimethylsilyl bis(amidinate)actinide complexes: synthesis and reactivity towards oxygen containing substrates. |
| Authors of publication | Karmel, Isabell S. R.; Elkin, Tatyana; Fridman, Natalia; Eisen, Moris S. |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2014 |
| Journal volume | 43 |
| Journal issue | 29 |
| Pages of publication | 11376 - 11387 |
| a | 19.515 ± 0.0004 Å |
| b | 10.564 ± 0.0002 Å |
| c | 22.454 ± 0.0004 Å |
| α | 90° |
| β | 109.196 ± 0.0009° |
| γ | 90° |
| Cell volume | 4371.66 ± 0.15 Å3 |
| Cell temperature | 240 ± 2 K |
| Ambient diffraction temperature | 240 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0538 |
| Residual factor for significantly intense reflections | 0.0317 |
| Weighted residual factors for significantly intense reflections | 0.0692 |
| Weighted residual factors for all reflections included in the refinement | 0.0759 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.028 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 180018 (current) | 2016-03-25 | cif/7/03/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/03/12. |
7031299.cif |
| 119463 | 2014-07-07 | cif/ Updating files of 7031298, 7031299, 7031300, 7031301 Original log message: Adding full bibliography for 7031298--7031301.cif. |
7031299.cif |
| 116352 | 2014-06-10 | cif/ Adding structures of 7031298, 7031299, 7031300, 7031301 via cif-deposit CGI script. |
7031299.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.