Crystallography Open Database

Information card for entry 7032584

Preview

Coordinates	7032584.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C49.5 H49.5 Cu3 N10 O18
Calculated formula	C49.5 H49.5 Cu3 N10 O18
Title of publication	Discrete and polymeric Cu(ii) complexes featuring substituted indazole ligands: their synthesis and structural chemistry.
Authors of publication	Hawes, Chris S.; Kruger, Paul E.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	43
Pages of publication	16450 - 16458
a	10.2213 ± 0.0006 Å
b	11.4215 ± 0.0005 Å
c	14.0872 ± 0.0007 Å
α	105.934 ± 0.004°
β	101.559 ± 0.004°
γ	104.354 ± 0.004°
Cell volume	1467.04 ± 0.15 Å³
Cell temperature	120 ± 1 K
Ambient diffraction temperature	120 ± 1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0624
Residual factor for significantly intense reflections	0.0549
Weighted residual factors for significantly intense reflections	0.155
Weighted residual factors for all reflections included in the refinement	0.1646
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7032584.cif
126451	2014-11-06	cif/ Updating files of 7032579, 7032580, 7032581, 7032582, 7032583, 7032584, 7032585 Original log message: Adding full bibliography for 7032579--7032585.cif.	7032584.cif
123907	2014-09-17	cif/ Adding structures of 7032579, 7032580, 7032581, 7032582, 7032583, 7032584, 7032585 via cif-deposit CGI script.	7032584.cif