Crystallography Open Database

Information card for entry 7033633

Preview

Coordinates	7033633.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[V2(PS3")2(mu-Se2)(mu-Se)]
Formula	C57.4 H72 O0.85 P2 S6 Se3 Si6 V2
Calculated formula	C57.4 H72 O0.85 P2 S6 Se3 Si6 V2
Title of publication	Non-oxido divanadium(iv) and divanadium(v) thiolate complexes with a new type of chalcogenide bridging motif.
Authors of publication	Wu, Hong-Ming; Chang, Ya-Ho; Tsai, Yi-Fang; Hsu, Kuei-Fang; Lee, Gene-Hsiang; Hsu, Hua-Fen
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	10
Pages of publication	4468 - 4473
a	15.43 ± 0.002 Å
b	15.527 ± 0.002 Å
c	17.671 ± 0.002 Å
α	80.054 ± 0.002°
β	69.489 ± 0.002°
γ	77.016 ± 0.002°
Cell volume	3843.3 ± 0.8 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1733
Residual factor for significantly intense reflections	0.0659
Weighted residual factors for significantly intense reflections	0.1654
Weighted residual factors for all reflections included in the refinement	0.2082
Goodness-of-fit parameter for all reflections included in the refinement	0.974
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7033633.cif
133312	2015-03-06	cif/ Updating files of 7033631, 7033632, 7033633, 7033634 Original log message: Adding full bibliography for 7033631--7033634.cif.	7033633.cif
129667	2015-01-15	cif/ Adding structures of 7033631, 7033632, 7033633, 7033634 via cif-deposit CGI script.	7033633.cif