Crystallography Open Database

Information card for entry 7034061

Preview

Coordinates	7034061.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H50 B N O2 P2 S Si Yb
Calculated formula	C36 H50 B N O2 P2 S Si Yb
Title of publication	(Iminophosphoranyl)(thiophosphoranyl)methane rare-earth borohydride complexes: synthesis, structures and polymerization catalysis.
Authors of publication	Schmid, Matthias; Oña-Burgos, Pascual; Guillaume, Sophie M.; Roesky, Peter W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	27
Pages of publication	12338 - 12348
a	9.7136 ± 0.0004 Å
b	13.3724 ± 0.0006 Å
c	15.3575 ± 0.0007 Å
α	91.806 ± 0.004°
β	103.465 ± 0.003°
γ	97.606 ± 0.003°
Cell volume	1918.92 ± 0.15 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0475
Residual factor for significantly intense reflections	0.0333
Weighted residual factors for significantly intense reflections	0.0813
Weighted residual factors for all reflections included in the refinement	0.0869
Goodness-of-fit parameter for all reflections included in the refinement	1.043
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180046 (current)	2016-03-25	cif/7/03/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/03/40.	7034061.cif
143634	2015-07-11	cif/ Updating files of 7034061, 7034062, 7034063, 7034064, 7034065, 7034066, 7034067, 7034068 Original log message: Adding full bibliography for 7034061--7034068.cif.	7034061.cif
131908	2015-02-17	cif/ Adding structures of 7034061, 7034062, 7034063, 7034064, 7034065, 7034066, 7034067, 7034068 via cif-deposit CGI script.	7034061.cif