Crystallography Open Database

Information card for entry 7034303

Preview

Coordinates	7034303.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H64 Cl3 Li N2 O2 Si Zr
Calculated formula	C38 H64 Cl3 Li N2 O2 Si Zr
Title of publication	Synthesis, characterisation, and dehydrocoupling ability of zirconium complexes bearing hindered bis(amido)silyl ligands.
Authors of publication	Lummis, Paul A.; McDonald, Robert; Ferguson, Michael J.; Rivard, Eric
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	15
Pages of publication	7009 - 7020
a	10.2481 ± 0.0004 Å
b	27.2915 ± 0.0011 Å
c	15.7628 ± 0.0006 Å
α	90°
β	101.817 ± 0.0004°
γ	90°
Cell volume	4315.2 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0423
Residual factor for significantly intense reflections	0.0379
Weighted residual factors for significantly intense reflections	0.0961
Weighted residual factors for all reflections included in the refinement	0.0989
Goodness-of-fit parameter for all reflections included in the refinement	1.112
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180049 (current)	2016-03-25	cif/7/03/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/03/43.	7034303.cif
134985	2015-04-06	cif/ Updating files of 7034303, 7034304, 7034305, 7034306, 7034307, 7034308 Original log message: Adding full bibliography for 7034303--7034308.cif.	7034303.cif
133596	2015-03-07	cif/ Adding structures of 7034303, 7034304, 7034305, 7034306, 7034307, 7034308 via cif-deposit CGI script.	7034303.cif