Crystallography Open Database

Information card for entry 7035059

Preview

Coordinates	7035059.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	GW
Formula	C47 H56 F6 O P4 Pt
Calculated formula	C47 H56 F6 O P4 Pt
Title of publication	Synthesis of a phosphapyracene via metal-mediated cyclization: structural and reactivity effects of acenaphthene precursors.
Authors of publication	Wang, Ge; Guino-O, Marites A; Glueck, David S.; Golen, James A.; Daley, Christopher J. A.; Rheingold, Arnold L.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	21
Pages of publication	9943 - 9954
a	11.5207 ± 0.0004 Å
b	17.2787 ± 0.0005 Å
c	22.7156 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	4521.8 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0462
Residual factor for significantly intense reflections	0.0438
Weighted residual factors for significantly intense reflections	0.0684
Weighted residual factors for all reflections included in the refinement	0.0719
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
138694 (current)	2015-06-07	cif/ Updating files of 7035053, 7035054, 7035055, 7035056, 7035057, 7035058, 7035059, 7035060, 7035061, 7035062 Original log message: Adding full bibliography for 7035053--7035062.cif.	7035059.cif
135928	2015-05-09	cif/ Adding structures of 7035053, 7035054, 7035055, 7035056, 7035057, 7035058, 7035059, 7035060, 7035061, 7035062 via cif-deposit CGI script.	7035059.cif