Crystallography Open Database

Information card for entry 7035421

Preview

Coordinates	7035421.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H36 Cl14 Ga4 N4 P10 Si5
Calculated formula	C12 H36 Cl14 Ga4 N4 P10 Si5
Title of publication	Formation of the spirocyclic, Si-centered cage cations [ClP(NSiMe3)2Si(NSiMe3)2P5](+) and [P5(NSiMe3)2Si(NSiMe3)2P5](2.).
Authors of publication	Holthausen, M. H.; Weigand, J. J.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	5
Pages of publication	1953 - 1961
a	9.9999 ± 0.0001 Å
b	23.7473 ± 0.0003 Å
c	26.3333 ± 0.0003 Å
α	63.844 ± 0.001°
β	79.463 ± 0.001°
γ	86.969 ± 0.001°
Cell volume	5515.64 ± 0.12 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0683
Residual factor for significantly intense reflections	0.0468
Weighted residual factors for significantly intense reflections	0.1074
Weighted residual factors for all reflections included in the refinement	0.1208
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176093 (current)	2016-02-05	cif/ Updating files of 7035419, 7035420, 7035421, 7035422 Original log message: Adding full bibliography for 7035419--7035422.cif.	7035421.cif
139245	2015-06-16	cif/ Adding structures of 7035419, 7035420, 7035421, 7035422 via cif-deposit CGI script.	7035421.cif