Crystallography Open Database

Information card for entry 7035822

Preview

Coordinates	7035822.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	[K(18-crown-6)]2[P7Ge{N(SiMe3)2}]*2py
Formula	C40 H76 Ge K2 N3 O12 P7 Si2
Calculated formula	C40 H76 Ge K2 N3 O12 P7 Si2
Title of publication	Heptaphosphide cluster anions bearing group 14 element amide functionalities.
Authors of publication	Quintero, Gabriela Espinoza; Paterson-Taylor, Isabelle; Rees, Nicholas H.; Goicoechea, Jose M.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	5
Pages of publication	1930 - 1936
a	13.081 ± 0.0002 Å
b	15.6526 ± 0.0003 Å
c	15.7164 ± 0.0003 Å
α	87.749 ± 0.001°
β	72.748 ± 0.001°
γ	77.053 ± 0.001°
Cell volume	2993.78 ± 0.1 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0576
Residual factor for significantly intense reflections	0.0393
Weighted residual factors for significantly intense reflections	0.0955
Weighted residual factors for all reflections included in the refinement	0.1057
Goodness-of-fit parameter for all reflections included in the refinement	1.006
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176062 (current)	2016-02-05	cif/ Updating files of 7035822, 7035823 Original log message: Adding full bibliography for 7035822--7035823.cif.	7035822.cif
152278	2015-07-18	cif/ Adding structures of 7035822, 7035823 via cif-deposit CGI script.	7035822.cif