Crystallography Open Database

Information card for entry 7035850

Preview

Coordinates	7035850.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H54 Cu N4 P Si2
Calculated formula	C32 H54 Cu N4 P Si2
Title of publication	Enhanced thermal stability of Cu-silylphosphido complexes via NHC ligation.
Authors of publication	Khalili Najafabadi, Bahareh; Corrigan, John F.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	32
Pages of publication	14235 - 14241
a	9.611 ± 0.004 Å
b	20.206 ± 0.008 Å
c	20.631 ± 0.006 Å
α	102.042 ± 0.013°
β	89.995 ± 0.009°
γ	96.848 ± 0.008°
Cell volume	3889 ± 3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1476
Residual factor for significantly intense reflections	0.128
Weighted residual factors for significantly intense reflections	0.331
Weighted residual factors for all reflections included in the refinement	0.3411
Goodness-of-fit parameter for all reflections included in the refinement	1.323
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
153217 (current)	2015-08-08	cif/ Updating files of 7035850, 7035851, 7035852, 7035853 Original log message: Adding full bibliography for 7035850--7035853.cif.	7035850.cif
152280	2015-07-18	cif/ Adding structures of 7035850, 7035851, 7035852, 7035853 via cif-deposit CGI script.	7035850.cif