Crystallography Open Database

Information card for entry 7036037

Preview

Structure parameters

Formula	C52 H58 Cl Mg N2 O P
Calculated formula	C52 H58 Cl Mg N2 O P
Title of publication	Reduction of dichloro(diaza-phospha)stibanes - isolation of a donor-stabilized distibenium dication.
Authors of publication	Hinz, Alexander; Rothe, Julia; Schulz, Axel; Villinger, Alexander
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	14
Pages of publication	6044 - 6052
a	12.8983 ± 0.0009 Å
b	15.7209 ± 0.0011 Å
c	22.3241 ± 0.0015 Å
α	90°
β	95.003 ± 0.004°
γ	90°
Cell volume	4509.5 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0973
Residual factor for significantly intense reflections	0.0523
Weighted residual factors for significantly intense reflections	0.1242
Weighted residual factors for all reflections included in the refinement	0.1489
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
301849 (current)	2025-08-21	Add cross-references to PubChem compounds in COD range 7/03/ Each referenced PubChem compound corresponds to the full crystal structure.	7036037.cif
181722	2016-04-05	cif/ Updating files of 7036034, 7036035, 7036036, 7036037, 7036038, 7036039 Original log message: Adding full bibliography for 7036034--7036039.cif.	7036037.cif
152717	2015-08-04	cif/ Adding structures of 7036034, 7036035, 7036036, 7036037, 7036038, 7036039 via cif-deposit CGI script.	7036037.cif