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Information card for entry 7036328
Preview
| Coordinates | 7036328.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H47 P Si2 |
|---|---|
| Calculated formula | C24 H47 P Si2 |
| Title of publication | Synthetic strategies to bicyclic tetraphosphanes using P1, P2 and P4 building blocks. |
| Authors of publication | Bresien, Jonas; Faust, Kirill; Hering-Junghans, Christian; Rothe, Julia; Schulz, Axel; Villinger, Alexander |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2016 |
| Journal volume | 45 |
| Journal issue | 5 |
| Pages of publication | 1998 - 2007 |
| a | 9.3749 ± 0.0006 Å |
| b | 16.9528 ± 0.0011 Å |
| c | 17.6869 ± 0.001 Å |
| α | 90° |
| β | 101.224 ± 0.003° |
| γ | 90° |
| Cell volume | 2757.2 ± 0.3 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0974 |
| Residual factor for significantly intense reflections | 0.0475 |
| Weighted residual factors for significantly intense reflections | 0.0979 |
| Weighted residual factors for all reflections included in the refinement | 0.1154 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.002 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176428 (current) | 2016-02-13 | Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively. |
7036328.cif |
| 176073 | 2016-02-05 | cif/ Updating files of 7036321, 7036322, 7036323, 7036324, 7036325, 7036326, 7036327, 7036328 Original log message: Adding full bibliography for 7036321--7036328.cif. |
7036328.cif |
| 153780 | 2015-08-29 | cif/ Adding structures of 7036321, 7036322, 7036323, 7036324, 7036325, 7036326, 7036327, 7036328 via cif-deposit CGI script. |
7036328.cif |
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Users of the data should acknowledge the original authors of the
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