Crystallography Open Database

Information card for entry 7036779

Preview

Coordinates	7036779.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C78.24 H108.49 Nb2 O6 P6 Sn
Calculated formula	C78.243 H108.486 Nb2 O6 P6 Sn
Title of publication	Assembly and stabilization of {E(cyclo-P3)2} (E = Sn, Pb) as a bridging ligand spanning two triaryloxyniobium units.
Authors of publication	Velian, Alexandra; Cossairt, Brandi M.; Cummins, Christopher C.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	5
Pages of publication	1891 - 1895
a	19.234 ± 0.002 Å
b	20.735 ± 0.002 Å
c	20.601 ± 0.002 Å
α	90°
β	92.989 ± 0.002°
γ	90°
Cell volume	8204.9 ± 1.4 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0656
Residual factor for significantly intense reflections	0.0364
Weighted residual factors for significantly intense reflections	0.0692
Weighted residual factors for all reflections included in the refinement	0.0796
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	7036779.cif
176068	2016-02-05	cif/ Updating files of 7036776, 7036777, 7036778, 7036779, 7036780, 7036781 Original log message: Adding full bibliography for 7036776--7036781.cif.	7036779.cif
160979	2015-10-08	cif/ Adding structures of 7036776, 7036777, 7036778, 7036779, 7036780, 7036781 via cif-deposit CGI script.	7036779.cif