Crystallography Open Database

Information card for entry 7036914

Preview

Coordinates	7036914.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H14 B F18 N
Calculated formula	C25 H14 B F18 N
Title of publication	Synthesis of 2-(lutidinyl)organoboranes and their reactivities against dihydrogen and pinacol borane.
Authors of publication	Zheng, Junhao; Lin, Yue-Jian; Wang, Huadong
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	14
Pages of publication	6088 - 6093
a	13.187 ± 0.002 Å
b	12.091 ± 0.002 Å
c	17.222 ± 0.003 Å
α	90°
β	110.411 ± 0.003°
γ	90°
Cell volume	2573.5 ± 0.7 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0693
Residual factor for significantly intense reflections	0.0493
Weighted residual factors for significantly intense reflections	0.1481
Weighted residual factors for all reflections included in the refinement	0.1668
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
181739 (current)	2016-04-05	cif/ Updating files of 7036908, 7036909, 7036910, 7036911, 7036912, 7036913, 7036914 Original log message: Adding full bibliography for 7036908--7036914.cif.	7036914.cif
169403	2015-10-21	cif/ Adding structures of 7036908, 7036909, 7036910, 7036911, 7036912, 7036913, 7036914 via cif-deposit CGI script.	7036914.cif