Crystallography Open Database

Information card for entry 7037133

Preview

Coordinates	7037133.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C15 H21 Cl6 Cu F6 N6 P2
Calculated formula	C15 H21 Cl6 Cu F6 N6 P2
Title of publication	Tris(pyrazolyl)phosphines with copper(i): from monomers to polymers.
Authors of publication	Tazelaar, Cornelis G. J.; Nicolas, Emmanuel; van Dijk, Tom; Broere, Daniël L J; Cardol, Mitchel; Lutz, Martin; Gudat, Dietrich; Slootweg, J. Chris; Lammertsma, Koop
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	5
Pages of publication	2237 - 2249
a	21.2337 ± 0.0005 Å
b	21.2337 ± 0.0005 Å
c	10.6155 ± 0.0004 Å
α	90°
β	90°
γ	120°
Cell volume	4145 ± 0.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	159
Hermann-Mauguin space group symbol	P 3 1 c
Hall space group symbol	P 3 -2c
Residual factor for all reflections	0.0627
Residual factor for significantly intense reflections	0.0462
Weighted residual factors for significantly intense reflections	0.11
Weighted residual factors for all reflections included in the refinement	0.1176
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176061 (current)	2016-02-05	cif/ Updating files of 7037130, 7037131, 7037132, 7037133, 7037134, 7037135 Original log message: Adding full bibliography for 7037130--7037135.cif.	7037133.cif
170234	2015-11-12	cif/ Adding structures of 7037130, 7037131, 7037132, 7037133, 7037134, 7037135 via cif-deposit CGI script.	7037133.cif