Crystallography Open Database

Information card for entry 7037143

Preview

Coordinates	7037143.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	[Os(bpy)2(dppcb)Pd(bpy)](PF6)4
Formula	C174 H151 F48 N17 Os2 P16 Pd2
Calculated formula	C174 H151 F48 N17 Os2 P16 Pd2
Title of publication	Unusual stability of dyads during photochemical hydrogen production.
Authors of publication	Prock, J.; Strabler, C.; Viertl, W.; Kopacka, H.; Obendorf, D.; Müller, T; Tordin, E.; Salzl, S.; Knör, G; Mauro, M.; De Cola, L.; Brüggeller, P
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	48
Pages of publication	20936 - 20948
a	14.0903 ± 0.0002 Å
b	17.957 ± 0.0003 Å
c	20.4371 ± 0.0003 Å
α	72.727 ± 0.0008°
β	88.1416 ± 0.0009°
γ	89.5445 ± 0.0008°
Cell volume	4935.17 ± 0.13 Å³
Cell temperature	243 ± 2 K
Ambient diffraction temperature	243 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0532
Residual factor for significantly intense reflections	0.0437
Weighted residual factors for significantly intense reflections	0.1241
Weighted residual factors for all reflections included in the refinement	0.1424
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
171144 (current)	2015-12-09	cif/ Updating files of 7037143, 7037144, 7037145 Original log message: Adding full bibliography for 7037143--7037145.cif.	7037143.cif
170237	2015-11-12	cif/ Adding structures of 7037143, 7037144, 7037145 via cif-deposit CGI script.	7037143.cif