Crystallography Open Database

Information card for entry 7037208

Preview

Coordinates	7037208.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54 H66 Mn Mo8 N12 O44
Calculated formula	C54 H66 Mn Mo8 N12 O44
Title of publication	Solvent-induced Mn(ii)/Zn(ii)/Co(ii) organopolymolybdate compounds constructed by bis-pyridyl-bis-amide ligands through the Mo-N bond: synthesis, structures and properties.
Authors of publication	Xu, Na; Zhang, Ju-Wen; Wang, Xiu-Li; Liu, Guo-Cheng; Li, Tian-Jiao
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	45
Journal issue	2
Pages of publication	760 - 767
a	11.7431 ± 0.001 Å
b	13.2703 ± 0.001 Å
c	13.7193 ± 0.0011 Å
α	107.661 ± 0.001°
β	106.897 ± 0.001°
γ	95.669 ± 0.002°
Cell volume	1907.8 ± 0.3 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0799
Residual factor for significantly intense reflections	0.0447
Weighted residual factors for significantly intense reflections	0.0989
Weighted residual factors for all reflections included in the refinement	0.1137
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
175983 (current)	2016-02-05	cif/ Updating files of 7037208, 7037209, 7037210 Original log message: Adding full bibliography for 7037208--7037210.cif.	7037208.cif
170292	2015-11-14	cif/ Adding structures of 7037208, 7037209, 7037210 via cif-deposit CGI script.	7037208.cif