Crystallography Open Database

Information card for entry 7037290

Preview

Coordinates	7037290.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H30 O3 Si3
Calculated formula	C24 H30 O3 Si3
SMILES	[Si]1(OC)(C[Si](OC)(C[Si](OC)(C1)c1ccccc1)c1ccccc1)c1ccccc1
Title of publication	Tridentate Lewis acids with phenyl substituted 1,3,5-trisilacyclohexane backbones.
Authors of publication	Weisheim, Eugen; Bücker, Lisa; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	45
Journal issue	1
Pages of publication	198 - 207
a	9.64716 ± 0.00011 Å
b	21.6495 ± 0.0002 Å
c	11.66228 ± 0.00013 Å
α	90°
β	91.649 ± 0.001°
γ	90°
Cell volume	2434.73 ± 0.04 Å³
Cell temperature	99.99 ± 0.1 K
Ambient diffraction temperature	99.99 ± 0.1 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0347
Residual factor for significantly intense reflections	0.0324
Weighted residual factors for significantly intense reflections	0.0861
Weighted residual factors for all reflections included in the refinement	0.0874
Goodness-of-fit parameter for all reflections included in the refinement	1.122
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176115 (current)	2016-02-05	cif/ Updating files of 7037290, 7037291, 7037292, 7037293 Original log message: Adding full bibliography for 7037290--7037293.cif.	7037290.cif
170383	2015-11-18	cif/ Adding structures of 7037290, 7037291, 7037292, 7037293 via cif-deposit CGI script.	7037290.cif