Crystallography Open Database

Information card for entry 7037292

Preview

Coordinates	7037292.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H24 Si3
Calculated formula	C21 H24 Si3
SMILES	[SiH]1(C[SiH](C[SiH](C1)c1ccccc1)c1ccccc1)c1ccccc1
Title of publication	Tridentate Lewis acids with phenyl substituted 1,3,5-trisilacyclohexane backbones.
Authors of publication	Weisheim, Eugen; Bücker, Lisa; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	45
Journal issue	1
Pages of publication	198 - 207
a	10.5439 ± 0.0003 Å
b	13.7178 ± 0.0007 Å
c	14.6783 ± 0.0006 Å
α	94.574 ± 0.004°
β	100.085 ± 0.003°
γ	100.821 ± 0.004°
Cell volume	2039.11 ± 0.15 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1046
Residual factor for significantly intense reflections	0.0516
Weighted residual factors for significantly intense reflections	0.1225
Weighted residual factors for all reflections included in the refinement	0.1338
Goodness-of-fit parameter for all reflections included in the refinement	0.894
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176115 (current)	2016-02-05	cif/ Updating files of 7037290, 7037291, 7037292, 7037293 Original log message: Adding full bibliography for 7037290--7037293.cif.	7037292.cif
170383	2015-11-18	cif/ Adding structures of 7037290, 7037291, 7037292, 7037293 via cif-deposit CGI script.	7037292.cif