Crystallography Open Database

Information card for entry 7037441

Preview

Coordinates	7037441.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H25 O3 P
Calculated formula	C33 H25 O3 P
Title of publication	The design of second generation MOP-phosphonites: efficient chiral hydrosilylation of functionalised styrenes.
Authors of publication	Fleming, James T.; Ficks, Arne; Waddell, Paul G.; Harrington, Ross W.; Higham, Lee J.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	5
Pages of publication	1886 - 1890
a	10.5786 ± 0.00007 Å
b	16.52575 ± 0.00009 Å
c	14.80544 ± 0.00008 Å
α	90°
β	95.7963 ± 0.0006°
γ	90°
Cell volume	2575.04 ± 0.03 Å³
Cell temperature	150 ± 0.2 K
Ambient diffraction temperature	150 ± 0.2 K
Number of distinct elements	4
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0303
Residual factor for significantly intense reflections	0.0273
Weighted residual factors for significantly intense reflections	0.0645
Weighted residual factors for all reflections included in the refinement	0.0663
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176099 (current)	2016-02-05	cif/ Updating files of 7037441, 7037442, 7037443, 7037444 Original log message: Adding full bibliography for 7037441--7037444.cif.	7037441.cif
170532	2015-11-25	cif/ Adding structures of 7037441, 7037442, 7037443, 7037444 via cif-deposit CGI script.	7037441.cif