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Information card for entry 7038487
Preview
| Coordinates | 7038487.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C33 H54 Bi N3 Si3 |
|---|---|
| Calculated formula | C33 H54 Bi N3 Si3 |
| SMILES | [Bi](N([Si](C)(C)C)c1cc(c(cc1)C)C)(N([Si](C)(C)C)c1cc(c(cc1)C)C)N([Si](C)(C)C)c1cc(c(cc1)C)C |
| Title of publication | Synthesis of mono-, di-, and triaminobismuthanes and observation of C-C coupling of aromatic systems with bismuth(iii) chloride. |
| Authors of publication | Hering-Junghans, Christian; Schulz, Axel; Thomas, Max; Villinger, Alexander |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2016 |
| Journal volume | 45 |
| Journal issue | 14 |
| Pages of publication | 6053 - 6059 |
| a | 11.1196 ± 0.0004 Å |
| b | 17.8846 ± 0.0007 Å |
| c | 18.8099 ± 0.0007 Å |
| α | 90° |
| β | 91.798 ± 0.002° |
| γ | 90° |
| Cell volume | 3738.9 ± 0.2 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0866 |
| Residual factor for significantly intense reflections | 0.0426 |
| Weighted residual factors for significantly intense reflections | 0.0723 |
| Weighted residual factors for all reflections included in the refinement | 0.0825 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.018 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181736 (current) | 2016-04-05 | cif/ Updating files of 7038481, 7038482, 7038483, 7038484, 7038485, 7038486, 7038487, 7038488, 7038489, 7038490, 7038491, 7038492, 7038493, 7038494, 7038495, 7038496, 7038497, 7038498, 7038499 Original log message: Adding full bibliography for 7038481--7038499.cif. |
7038487.cif |
| 176784 | 2016-02-20 | cif/ Adding structures of 7038481, 7038482, 7038483, 7038484, 7038485, 7038486, 7038487, 7038488, 7038489, 7038490, 7038491, 7038492, 7038493, 7038494, 7038495, 7038496, 7038497, 7038498, 7038499 via cif-deposit CGI script. |
7038487.cif |
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Users of the data should acknowledge the original authors of the
structural data.